Page 64 <br />Section I: Tact-uvic~u. SBxvicas <br />LABORATORY <br />The laboratory provides daily analytical monitor- <br />ing of plant wastewater to ensure the plant is in <br />compliance with federal, state, and local require- <br />ments. The labo- <br />ratory also assists <br />the Operations <br />Section with <br />plantprocesscon- <br />trolanalyses,asre- <br />quested, and per- <br />forms analyses as <br />neededforspecial <br />projects and for <br />otherCitydepart- <br />ments. The labo- <br />ratory also per- <br />forms analytical <br />services for indus- <br />trial waste moni- <br />toring, for the <br />Sludge Manage- <br />ment program, <br />and for the Can- <br />neryWaste Man- <br />agement Facility. <br />The laboratory <br />performs 14>000 <br />analyses and tests <br />500 wells each <br />STAFFING <br />year. <br />Since plant start-up, laboratory staff has increased <br />from a supervisor and two technicians to a supervi- <br />sor, an environmental analyst, four technicians, <br />two journeymen (Technician III's), and two ap- <br />prentices (Technician II's). <br />The laboratory is staffed seven days a week with <br />one technician working weekends. Weekend duty <br />rotates among technicians every four weeks. <br />FACILITIES AND EQUIPMENT <br />The 2,300-square-foot analytical laboratory is lo- <br />cated inthe Administration Building and is shared <br />with the industrial monitoring staff. Following are <br />the major pieces of analytical equipment used by <br />the laboratory: <br />• Atomic Absorption <br />Spectrophotometer <br />This analyzer is a Perking Elmer 3030, with an <br />HGA 500 graphite furnace and autosampler and <br />MHS-10 mercury/hybride system. The spectro- <br />photometer isused toanalyzethe metals contained <br />in sludge, soil, plant wastewater, industrial waste, <br />cannery wastewater, and groundwater at the Sludge <br />Management Facility. <br />• Carbon Analyzer <br />The new carbon analyzer is a Dohrmann DC-80 <br />and is used primarily to analyze the total organic <br />carbon contained in cannery wastewater and the <br />groundwater at the Cannery Waste Management <br />Facility and the Sludge Management Facility. <br />• Block Digestion System <br />The Tecator Block Digestion System is used to <br />analyze total kj eldahl nitrogen in samples of sludge, <br />soil, groundwater, and cannery wastewater. <br />• Ion Analyzer <br />The Lachat Flow Injection Analysis Autoanalyzer <br />is used primarily to analyze samples of sludge, <br />groundwater, cannerywastewater, andplantwaste- <br />waterfor nitrates and chlorides. <br />DATA MANAGEMENT <br />The laboratory uses a PC-based laboratory infor- <br />mation system to handle data management. All <br />sample s, except for routine plant samples, are logged <br />into the system and recorded with sampling data, <br />preservative information, andtestingrequirements <br />when they arrive at the laboratory. When testing <br />is completed, labels are printed for the sample <br />containers, and reports are generated. The system <br />was designed by Wastewater Division staff using <br />dBase III software. <br />QUALITY ASSURANCE~QUALITY <br />CONTROL PROGRAM <br />A manual outlines the program and its require- <br />ments. Control charts are maintained whenever <br />possible andareoncomputerspreadsheets. A Labo- <br />ratoryProcedures Manual outlines standardproce- <br />duresfor performing routine analyses. <br />A technician performs metals analysis with the atomic <br />absorption spectrophotometer. <br />